Multiple Autoclaves / Parallel Synthesizer

Salient Features

  • 4 or 6 nos. of 50 ml to 2 ltr parallel overhead stirred autoclaves
  • Common mounting & control panel with remote monitoring & control
  • Pressures upto 350 bar & temperatures upto 500°C
  • Simultaneous reactions can be carried out in each reactor with different parameters & comparative studies can be done from the data received. It saves lot of space & helps in advanced & faster research i.e. high throughput testing
  • The optional accessories can be common or separate for all autoclaves

Standard models for Multiple Autoclaves

M4: 4 nos. autoclave in parallel
M6: 6 nos. autoclave in parallel

Standard models for 50 ml

Description M4 or M6
Model no. A 1213 A 1215 A 1223 A 1225 A 1233 A 1235
Design Pressure 100 bar 200 bar 350 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 40
Vessel Internal Height (mm) 63
Min. Stirrable Volume (ml) 20

Standard models for 100 ml

Description M4 or M6
Model no. A 1313 A 1315 A 1323 A 1325 A 1333 A 1335
Design Pressure 100 bar 200 bar 350 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 40
Vessel Internal Height (mm) 83
Min. Stirrable Volume (ml) 20

Standard models for 250 ml

Description M4 or M6
Model no. A 1413 A 1415 A 1423 A 1425 A 1433 A 1435
Design Pressure 100 bar 200 bar 350 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 65
Vessel Internal Height (mm) 80
Min. Stirrable Volume (ml) 50

Standard models for 500 ml

Description M4 or M6
Model no. A 2113 A 2115 A 2123 A 2125 A 2133 A 2135
Design Pressure 100 bar 200 bar 350 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 75 65
Vessel Internal Height (mm) 118 158
Min. Stirrable Volume (ml) 60 50

Standard models for 750 ml

Description M4 or M6
Model no. A 2213 A 2215 A 2223 A 2225 A 2233 A 2235
Design Pressure 100 bar 200 bar 350 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 75
Vessel Internal Height (mm) 193
Min. Stirrable Volume (ml) 60

Standard models for 1 ltr

Description M4 or M6
Model no. A 2313 A 2315 A 2323 A 2325 A 2333 A 2335
Design Pressure 100 bar 200 bar 350 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 101.6 75
Vessel Internal Height (mm) 163 273
Min. Stirrable Volume (ml) 130 60

Standard models for 2 ltr

Description M4 or M6
Model no. A 2413 A 2415 A 2423 A 2425 A 2433 A 2435
Design Pressure 100 bar 200 bar 350 bar
Design Temperature 300°C 500°C 300°C 500°C 300°C 500°C
Vessel I/D (mm) 101.6
Vessel Internal Height (mm) 303
Min. Stirrable Volume (ml) 130

Note: The above ratings are only for SS316, Hastelloy C & Inconel materials, for other materials the ratings will change depending on its stress value& maximum allowable temperature as per ASME code.

Technical specification for multiple autoclave standard models

Sr. Description Specification
A Material of Construction SS 316 wetted parts
B Head Mounting Style Removable head & vessel design
C Heating Type Electrical ceramic band heater with cladding & insulation & heater temperature control for 500°C
D Motor ⅛ hp AC motor with 100-1450 RPM((50 ml to 250 ml)
¼ hp AC motor with 100-1450 RPM((500 ml to 2 ltr)
E Shaft Sealing Zero leakage magnetic drive coupling M8 with 0.8 Nm torque for 50 ml to 250 ml & M20 with 2 Nm torque for 500 ml to 2 ltr
F Stirrer 4 bladed turbine stirrer (50 ml to 250 ml)
2 stage 6 bladed turbine stirrer(500 ml to 2 ltr)
G Standard Nozzles, Valves & Fittings External Valves & Fittings:
Pressure gauge, safety rupture disc, gas inlet and liquid sampling needle valve with commondip tube, vent needle valve, solenoid valve at inlet of cooling coil (50 ml to 250 ml)
Internal Fittings:
Serpentine cooling coil (50 ml to 250 ml), Helical cooling coil (500 ml to 2 ltr), dip tube, thermowell with RTD PT100 temperature sensor
H Gasket PTFE up to 300°C and metallic grafoil gasket up to 500°C
I Closure Type Split clamp with clamp bolts
J Control Panel SS control panel with programmable PID temperature controller with high temperature alarm andvariable frequency drive for motor speed control
K Power Supply 1Ø, 220 V AC, 50 / 60 Hz
L Mounting & Dimensions SS Table Top (50 ml to 1 ltr)
SS Trolley (2 ltr)

Enquiry guide for multiple autoclave customized models

Enquiry code structure is Standard Model no. A-B-C-D1-D2-D3-E-F-G-I-J-L-M where A, B, C, D1,D2, D3, E, F, G, I, J, L & M options can beselected from below tables. The below options will be in place of standard supply. For example 4 nos. of 500 ml, 100 bar, 300°C, Hastelloy C,fixed head autoclave with ATEX Zone1 certified, heater & motor will read as M4 2113-HC6-K-EZ-AZ

A Material of Construction
SS 316L 316L
Hastelloy C 276 HC6
Hastelloy C 22 HC2
Hastelloy B HB
Monel 400 MN4
Inconel 600 IN6
Inconel 625 IN5
Nickel 200 NK2
Titanium Gr. 2 TI2
Zirconium 702 ZR7
Tantalum TAN
Tantalum lined TNL
B Head Mounting Style
Fixed head with manual vessel raising lowering (50 ml & 750 ml) K
Fixed head with pneumatic vessel raising lowering (50 ml & 2 ltr) P
Fixed head with manual vessel raising lowering & tilting (50 ml & 750 ml)) KT
Fixed head with pneumatic vessel raising lowering & tilting (50 ml & 2 ltr) PT
C Heating Style
Electrical ex-proof, IIB + H2 certified EA
Electrical ex-proof ATEX Zone1 certified EZ
Electrical ex-proof Class 1 Div 2 EC
Welded SS 304 jacket with insulation JS
Welded SS 304 jacket with electrical ceramic heater JH
Peltier cooler for -25 to 150°C (for 50 ml to 250 ml) PL
D2 RPM
Upto 3000 rpm RT
Gear box up to 440 rpm R4
D3 Motor Type
Ex-proof gas group IIB (Zone 1) XB
Ex-proof gas group IIC (Zone 1) XC
Ex-proof CE ATEX certified II 2G Ex de IIC T4 AZ
Ex-proof CSA certified Class 1 Div 2 group A, B, C, D CD
⅛ hp compact in-line brushless DC motor BD
¼ hp compact in-line brushless DC motor QD
E Mag Drive Torque
2 Nm (for 50 ml to 250 ml) M20
4 Nm (for 500 m to 2 ltr) M40
8 Nm (for 500 m to 2 ltr) M80
12 Nm (for 1 ltr to 2 ltr) M120
F Stirrer Options*
Hollow shaft with gas induction Impeller SH
Anchor (Serpentine cooling coil, max 100 rpm) SA
Spiral (No cooling coil, max 100 rpm) SS
Ruston turbine SR
Paddle SD
Propeller SP
G Valves & Fittings**
Serpentine cooling coil SCC
Ball valve powder inlet (¼) with funnel BVP
Flush bottom valve (10 mm) FBV
Baffle (with serpentine cooling coil) BFL
I Closure Type
Threaded cap with 'O' ring FKM (Viton) up to 225°C CV
Threaded cap with 'O'ring FFKM (Kalrez) up to 275°C CK
Split clamp with 'O' ring FKM (Viton) up to 225°C SV
Split clamp with 'O'ring FFKM (FFKM (Kalrez) up to 275°C SK
J Control Panel
Touch screen-HMI panel TSP
L Mounting & Overall Dimensions (WxDxH)
SS Trolley (50 ml to 1 ltr) TL
M Certifications***
Design approval as per ASME code by notified body DAC
CE-PED 2014/68/EU PED
ASME U/U2 stamp coded ASU
ATEX certified reactor 2014/34/EU ASA
CE marked panel & electrical parts ECE
UL/CSA marked panel & electrical parts USC
Notes:
  1. Customer is advised to select best suited options for most optimized price & delivery.
  2. For other optional accessories please refer Accessories tab
  3. All above options may not be available / possible with all models.
  4. Customization of volume, material, pressure, temperature etc. may be possible on request.
  5. Different power supply options may be possible on request.
  6. Overall dimensions are indicative, they may change depending on the optional accessories or specific design modifications opted.
  7. * Stirrer options can be in place of standard or additional multiple interchangeable.
  8. **All option specified in G are addons & multiple/ all of them can be availed at the same time.
  9. *** Country specific certification like CRN for Canada, AS1210 for Australia & DOSH for Malaysia can be offered on request.

Optional Accessories

MAGNA-SAFE INTERNATIONAL
P.O.BOX 447
OLD BRIDGE, NJ 08857-0447

 ( 866 ) 626 8885

  www.magnasafe.com

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